SEM Facility for Examination of Reactive and Radioactive Materials

Archive description

A scanning electron microscope (SEM) facility for the examination of tritium-containing materials is operational at Mound Laboratory. The SEM is installed with the sample chamber incorporated as an integral part of an inert gas glovebox facility to enable easy handling of radioactive and pyrophoric materials. A standard SEM (ETEC Model B-1) was modified to meet dimensional, operational, and safety-related requirements. A glovebox was designed and fabricated which permitted access with the gloves to all parts of the SEM sample chamber to facilitate detector and accessory replacement and repairs. A separate console combining the electron optical column and specimen chamber was interfaced to the glovebox by a custom-made, neoprene bellows so that the vibrations normally associated with the blowers and pumps were damped. Photomicrographs of tritiated pyrophoric materials show the usefulness of this facility. Some of the difficulties involved in the investigation of these materials are also discussed. The SEM is also equipped with an energy dispersive X-ray detector (ORTEC) and a Secondary Ion Mass Spectrometer (3M) attachments. This latter attachment allows analysis of secondary ions with masses ranging from 1-300 amu.